Preparative isolation and purification of geniposide from gardenia fruits by centrifugal partition chromatography
- Title
- Preparative isolation and purification of geniposide from gardenia fruits by centrifugal partition chromatography
- Author
- 김철영
- Keywords
- centrifugal partition chromatography; iridoid glycoside; geniposide; Gardenia jasminoides; Rubiaceae
- Issue Date
- 2007-03
- Publisher
- JOHN WILEY & SONS LTD
- Citation
- PHYTOCHEMICAL ANALYSIS, v. 18, No. 2, Page. 115-117
- Abstract
- The iridoid glycoside, geniposide was purified by centrifugal partition chromatography (CPC) with a two-phase solvent system composed of ethyl acetate:isopropanol:water (3:2:5, v/v) from an 80% methanolic extract of fruits of Gardenia jusminoides. Preparative CPC yielded 56.2 mg of geniposide in a one-step separation of 500 mg of extract, with a purity of 95% as determined by HPLC. Isolated gemposide was identified from its H-1-NMR, C-13-NMR and MS spectra. Copyright (c) 2007 John Wiley & Sons, Ltd.
- URI
- https://onlinelibrary.wiley.com/doi/abs/10.1002/pca.958https://repository.hanyang.ac.kr/handle/20.500.11754/106363
- ISSN
- 0958-0344
- DOI
- 10.1002/pca.958
- Appears in Collections:
- COLLEGE OF PHARMACY[E](약학대학) > PHARMACY(약학과) > Articles
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