회수된 Bi2Te3의 계면활성제에 따른 합성 및 성장 거동
- Title
- 회수된 Bi2Te3의 계면활성제에 따른 합성 및 성장 거동
- Other Titles
- The Preparation and Growth Mechanism of the Recovered Bi2Te3 Particles with Respect to Surfactants
- Author
- 좌용호
- Keywords
- Recovered Bi2Te3; Chemical reduction; Surfactant; Morphology control; Growth mechanism
- Issue Date
- 2017-04
- Publisher
- 한국분말야금학회
- Citation
- 한국분말야금학회지, v. 24, NO. 2, Page. 141-146
- Abstract
- Bi2Te3 powders are recovered by wet chemical reduction for waste n-type thermoelectric chips, and the recovered particles with different morphologies are prepared using various surfactants such as cetyltrimethylammonium bromide (CTAB), sodium dodecylbenzenesulfonate (SDBS), and ethylenediaminetetraacetic acid (EDTA). When citric acid is added as the surfactant, the shape of the aggregated particles shows no distinctive features. On the other hand, rod-shaped particles are formed in the sample with CTAB, and sheet-like particles are synthesized with the addition of SDBS. Further, particles with a tripod shape are observed when EDTA is added as the surfactant. The growth mechanism of the particle shapes depending on the surfactant is investigated, with a focus on the nucleation and growth phenomena. These results help to elucidate the intrinsic formation mechanism of the rod, plate, and tripod structures of the Bi2Te3 recovered by the wet reduction process.
- URI
- http://ejournal.kpmi.or.kr/journal/article.php?code=52333https://repository.hanyang.ac.kr/handle/20.500.11754/181445
- ISSN
- 1225-7591;2287-8173
- DOI
- 10.4150/KPMI.2017.24.2.141
- Appears in Collections:
- COLLEGE OF ENGINEERING SCIENCES[E](공학대학) > MATERIALS SCIENCE AND CHEMICAL ENGINEERING(재료화학공학과) > Articles
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