Synthesis and Characterization of Polymeric Acid-Doped Polyaniline Interpenetrating Polymer Networks
- Title
- Synthesis and Characterization of Polymeric Acid-Doped Polyaniline Interpenetrating Polymer Networks
- Author
- 이병주
- Keywords
- poly(2-acrylamido-2-methylpropane sulfonic acid); polyaniline; thermal properties; semi-IPN
- Issue Date
- 2006-03
- Publisher
- TAYLOR & FRANCIS INC
- Citation
- JOURNAL OF MACROMOLECULAR SCIENCE PART A-PURE AND APPLIED CHEMISTRY, v. 43, No. 3, Page. 497-505
- Abstract
- Polyaniline (PANI)/poly(2-acrylamido-2-methylpropane sulfonic acid) (PAMPS) semi-interpenetrating network polymers (semi-IPNs) were prepared using the simultaneous method. The formation and properties of the interpenetrating PANI/PAMPS semi-IPNs were investigated using Fourier transform infrared spectroscopy, X-ray diffraction, solid-state C-13-NMR, differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). The interaction of PAMPS with PANI as a polymeric acid dopant was also investigated. These semi-IPNs had a different microstructure compared to that of pure PANI. Packing structures and several decomposition steps were ordered for each semi-IPN, while pure PANI exhibits a single amorphous peak and one decomposition step. The NMR spectra show that these peaks broaden and shifted downfield in the semi-IPNs. A thermal reaction between PANI and PAMPS was observed using DSC and TGA, and the data from the two techniques are in agreement.
- URI
- https://www.tandfonline.com/doi/full/10.1080/10601320600575165https://repository.hanyang.ac.kr/handle/20.500.11754/107802
- ISSN
- 1060-1325
- DOI
- 10.1080/10601320600575165
- Appears in Collections:
- COLLEGE OF ENGINEERING SCIENCES[E](공학대학) > ELECTRICAL ENGINEERING(전자공학부) > Articles
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