Full metadata record
DC Field | Value | Language |
---|---|---|
dc.contributor.author | 최성철 | - |
dc.date.accessioned | 2019-11-26T02:05:56Z | - |
dc.date.available | 2019-11-26T02:05:56Z | - |
dc.date.issued | 2017-06 | - |
dc.identifier.citation | CERAMICS INTERNATIONAL, v. 43, no. 8, page. 5896-5900 | en_US |
dc.identifier.issn | 0272-8842 | - |
dc.identifier.issn | 1873-3956 | - |
dc.identifier.uri | https://www.sciencedirect.com/science/article/pii/S0272884217300809?via%3Dihub | - |
dc.identifier.uri | https://repository.hanyang.ac.kr/handle/20.500.11754/114455 | - |
dc.description.abstract | Sub-micro sized zirconium diboride (ZrB2) powders were successfully prepared via the boro/carbothermal reduction method using zirconium oxide and boron carbide as the primary raw materials. The prepared mixtures were thermally reacted at 1250 degrees C for 1 h. The optimized composition range containing the lowest oxide and carbide impurity, which was 0.14% of oxygen and 0.3% of carbon contents, was determined using crystallographic and elemental analysis. The particle size was reduced from 5 pm to 245 nm by the addition of B4C as a reductant within a composition range that maintained the highest purity. The morphology changed from faceted to angular hexagonal bar-like with a simultaneous growth in particle size. Changes in the particle structure were a result of the existing liquid B2O3 phase during the reaction. The 245-nm particles contained 12.1% oxygen content and 16.2% oxygen content for the 5-mu m particle in the circumstance in which limited oxides could be produced. | en_US |
dc.description.sponsorship | This work was supported by the National Research Foundation of Korea (NRF) grant funded by the Korean government (2014R1A2A1A11050220), and the Power Generation and Electricity Delivery of the Korea Institute of Energy Technology Evaluation and Planning (KETEP) grant funded by the Ministry of Trade, Industry and Energy, Korea (20142020103400). | en_US |
dc.language.iso | en_US | en_US |
dc.publisher | ELSEVIER SCI LTD | en_US |
dc.subject | Zirconium diboride | en_US |
dc.subject | Synthesis | en_US |
dc.subject | Purity | en_US |
dc.subject | Morphology | en_US |
dc.subject | Boron carbide reduction | en_US |
dc.title | Synthesis of sub-micro sized high purity zirconium diboride powder through carbothermal and borothermal reduction method | en_US |
dc.type | Article | en_US |
dc.relation.no | 8 | - |
dc.relation.volume | 43 | - |
dc.identifier.doi | 10.1016/j.ceramint.2017.01.068 | - |
dc.relation.page | 5896-5900 | - |
dc.relation.journal | CERAMICS INTERNATIONAL | - |
dc.contributor.googleauthor | An, Gye Seok | - |
dc.contributor.googleauthor | Han, Jin Soon | - |
dc.contributor.googleauthor | Hur, Jae Uk | - |
dc.contributor.googleauthor | Choi, Sung-Churl | - |
dc.relation.code | 2017001945 | - |
dc.sector.campus | S | - |
dc.sector.daehak | COLLEGE OF ENGINEERING[S] | - |
dc.sector.department | DIVISION OF MATERIALS SCIENCE AND ENGINEERING | - |
dc.identifier.pid | choi0505 | - |
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