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Preparative isolation of mangiferin from Anemarrhena asphodeloides rhizomes by centrifugal partition chromatography

Title
Preparative isolation of mangiferin from Anemarrhena asphodeloides rhizomes by centrifugal partition chromatography
Author
김철영
Keywords
centrifugal partition chromatography; Anemarrhena asphodeloides; preparative chromatography; mangiferin; xanthone glycoside
Issue Date
2006-06
Publisher
TAYLOR & FRANCIS INC
Citation
JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES, v. 29, No. 6, Page. 869-875
Abstract
Mangiferin was separated from rhizomes of Anemarrhena asphodeloides extract using centrifugal partition chromatography (CPC) with a two-phase solvent system composed of ethyl acetate-isopropanol-water (3:2:5, v/v). Mangiferin (22.5 mg) was successfully isolated from methanolic extracts (957 mg) in only one step, and the purity of isolated compound was determined to be over 95% by HPLC analysis. The structure of mangiferin was identified by H-1, C-13 NMR and ESI-MS spectral data analysis.
URI
https://www.tandfonline.com/doi/full/10.1080/10826070500531391http://repository.hanyang.ac.kr/handle/20.500.11754/108248
ISSN
1082-6076; 1520-572X
DOI
10.1080/10826070500531391
Appears in Collections:
COLLEGE OF PHARMACY[E](약학대학) > PHARMACY(약학과) > Articles
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